SBIR-STTR Award

In-Situ Electrospray Capture of Organic Bearing Particulates from Comets and Celestial Bodies
Award last edited on: 1/20/2024

Sponsored Program
SBIR
Awarding Agency
NASA : ARC
Total Award Amount
$845,261
Award Phase
2
Solicitation Topic Code
S1.07
Principal Investigator
Joseph J Bango Jr

Company Information

Connecticut Analytical Corporation (AKA: CAC~CAC Diagnostics)

696 Amity Road
Bethany, CT 06524
   (800) 831-028
   info@ctanalytical.com
   www.ctanalytical.com
Location: Single
Congr. District: 03
County: New Haven

Phase I

Contract Number: 80NSSC18P2034
Start Date: 7/27/2018    Completed: 2/15/2019
Phase I year
2018
Phase I Amount
$111,999
NASA has need for technologies that can enable sampling from asteroids and from depth in a comet nucleus, improved in-situ analysis of comets. It has been identified that there is also a requirement for improved dust environment measurements & particle analysis, small body resource identification, and/or quantification of potential small body resources (e.g., oxygen, water and other volatiles, hydrated minerals, carbon compounds, fuels, etc.). We propose to leverage past observations of the ability of electrospray ionization to capture and concentrate polar or polarizable trace species without damage, and combine that knowledge with recent discoveries in developing a hyper velocity ice-gun for NASA studies aimed at ice grain capture simulations. The phase I effort will focus on using the ice gun we created under prior NASA support, and add a novel electrospray cross-current element that creates a soft charging plume across a series of discrete deceleration aerogel plates that we believe will enable in-situ organic analysis capability previously unattainable on board a spacecraft using existing NASA mass spectrometer hardware. Potential NASA Applications The applications of the proposed technology for NASA include the means to employ MS to potentially non-destructively analyze organic trace species in ice grains traveling at hyper velocities of 5km/sec and above, simplifys the orbital mechanics required for sample interception.. The long flight time back to Earth results in significant discovery delays. With the proposed technology, NASA could perform in-situ organic analysis of incident ice grains in near real-time.. Potential Non-NASA Applications For Non-NASA applications, the technology being offered in this proposal include the potential for new methods of ambient pathogen capture and soft ionization for mass spectrometric analysis. In addition, other applications may include non-organic polar molecule charging suitable for thin layer deposition, chip fabrication, and other semiconductor uses.

Phase II

Contract Number: 80NSSC19C0158
Start Date: 8/14/2019    Completed: 8/13/2021
Phase II year
2019
Phase II Amount
$733,262
NASA has need for technologies that can enable sampling from asteroids and from depth in a comet nucleus, improved in-situ analysis of comets. It has been identified that there is also a requirement for improved dust environment measurements & particle analysis, small body resource identification, and/or quantification of potential small body resources (e.g., oxygen, water and other volatiles, hydrated minerals, carbon compounds, fuels, etc.). We propose to leverage past observations of the ability of electrospray ionization to capture and concentrate polar or polarizable trace species without damage, and combine that knowledge with recent discoveries in developing a hyper velocity ice-gun for NASA studies aimed at ice grain capture simulations. The phase I effort will focus on using the ice gun we created under prior NASA support, and add a novel electrospray cross-current element that creates a soft charging plume across a series of discrete deceleration mylar plates that we believe will enable in-situ organic analysis capability previously unattainable on board a spacecraft using existing NASA mass spectrometer hardware. Potential NASA Applications (Limit 1500 characters, approximately 150 words) This technology offers the means to employ mass spectrometry with comet tail sampling. The ability to non-destructively analyze organic trace species in ice grains traveling at hyper velocities of 5km/s and above, would simplify orbital mechanics for sample interception.The creation of multiply charged ions offers using existing MS instruments to look for organic macromolecules without increasing analyzer upmass, size, or power requirements. This allows in-situ analysis of incident ice grains in near real-time, with samples retained for return. Potential Non-NASA Applications (Limit 1500 characters, approximately 150 words) For Non-NASA applications, the technology being offered in this proposal include the potential for new methods of ambient pathogen capture and soft ionization for mass spectrometric analysis. In addition, other applications may include non-organic polar molecule charging suitable for thin layer deposition, chip fabrication, and other semiconductor uses.