SBIR-STTR Award

Synchrotron light sources and X-ray free electron lasers are now generating shorter pulses with more intense light than ever before possible, granting unparalleled access to new discoveries. X-ray detectors have not kept pace with these improvements. The field of soft x-ray detection is particularly behind in detector development due to low signal levels resulting from the lower energy x-rays and high vacuum requirements. Existing detectors are often not commercially available, and do not address the need for single photon counting, event counting, and high image resolution simultaneously. This technology gap prevents advancements in fields like time resolved photoemission or x-ray photon-correlation spectroscopy. The proposed program will advance the development of a novel coupled microchannel plate (MCP) - application specific integrated circuit (ASIC) soft x-ray detector (CAMP) for multi-event encoding soft x-ray experiments. Laboratory-level prototypes of the CAMP detector have demonstrated single photon sensitivity and ability to correlate 104 simultaneous events with < 2 ns time resolution using a Timepix3 ASIC. The technology exists in a laboratory setting, but is not widely available to the soft x-ray community as a whole. The proposed program will leverage the developments existing in the literature and investigate the feasibility of transitioning the technology to a commercial instrument. The primary objective of the proposed program is to leverage the laboratory research and development in the literature and define a program to produce a commercial prototype. This will be done through leveraging connections with the user community to define detector requirements, creating a knowledge base of existing laboratory prototypes, and Sydor’s experience commercializing similar x-ray detectors alongside the scientific community. Phase I will culminate in a conceptual design for a commercial prototype to be produced in Phase II along with a product road map for future product releases. A robust and commercially supported detector with the combined low signal amplification of an MCP and simultaneous event encoding ability of an ASIC will enable discovery in soft x-ray experiments not currently possible. Current commercial offerings often use indirect detection which limits temporal resolution, and are only capable of counting < 10 simultaneous events (multi-anode photomultiplier tubes). This proposed CAMP detector will provide good time resolution, < 10 µm spatial resolution with centroiding, and encoding of up to ~ 104 simultaneous single photon events, drastically improving scientist’s ability to collect data, and allowing greater insight into materials.

Synchrotron light sources and x-ray free electron lasers are now generating shorter pulses with more intense light than ever before possible, granting unparalleled access to new discoveries. X-ray detectors have not kept pace with these improvements. The field of soft x-ray detection is particularly lagging due to low signal levels resulting from the lower energy x-rays and high vacuum requirements. Existing detectors are often not commercially available, and do not address the need for single photon counting, event counting, and high image resolution simultaneously. This technology gap prevents advancements in fields like time resolved photoemission or x-ray photon-correlation spectroscopy. The proposed program will advance the development of a novel coupled microchannel plate (MCP) - application specific integrated circuit (ASIC) soft x-ray detector for multi-event encoding soft x-ray experiments. Laboratory prototypes of the detector demonstrated single photon sensitivity correlation of 104 simultaneous events with < 2 ns time resolution using a commercial ASIC. The technology exists in a laboratory setting but is not widely available to the soft x-ray community. The proposed program will leverage developments in the literature and begin transitioning the technology to a commercial instrument. During Phase I, a conceptual commercial design and preliminary product roadmap. Steps needed to bring existing laboratory level technology to a commercial level were scoped. The team identified a microchannel plate manufacturing partner and selected a commercially available application specific integrated circuit most suitable for user applications. In addition, a system architecture for the first commercial prototype based on existing detector technology at the small business. The system is composed of a backplane board suitable for connecting multiple ASICs packaged as sensors for the detector. The primary objective of the proposed program is to test a commercial prototype at a beamline or equivalent soft x-ray source. A system will be designed and built to accommodate an in-vacuum sensor assembly consisting of the integrated circuit and microchannel plate, design commercial level electronics, and readout architecture design. Electronics and readout systems include design and layout of front-end detector electronics, frame grabber cards, and a user interface. Input from potential customers and beamline scientists will be integrated into the design and future product roadmap throughout the process. A robust and commercially supported detector with the low signal amplification of a microchannel plate and simultaneous event encoding ability of a commercial integrated circuit will enable discovery in soft x- ray experiments not currently possible. Current commercial offerings often use indirect detection which limits temporal resolution and are only capable of counting < 10 simultaneous events (multi-anode photomultiplier tubes). This proposed detector will provide good time resolution, < 10 µm spatial resolution with centroiding, and encoding thousands of simultaneous single photon events, drastically improving scientist’s ability to collect data, and allowing greater insight into materials.