SBIR-STTR Award

Improved thin film multilayer coatings for thermal neutron guides
Award last edited on: 2/19/02

Sponsored Program
SBIR
Awarding Agency
DOE
Total Award Amount
$548,786
Award Phase
2
Solicitation Topic Code
-----

Principal Investigator
John H Bradshaw

Company Information

Opto-Line Associates Inc

265 Ballardvale Street
Wilmington, MA 01887
   (978) 658-7255
   N/A
   N/A
Location: Single
Congr. District: 06
County: Middlesex

Phase I

Contract Number: ----------
Start Date: 00/00/00    Completed: 00/00/00
Phase I year
1989
Phase I Amount
$48,786
Adding mirror and supermirror neutron guides to existing and proposed thermal neutron research facilities has great economic benefits. Recent developments in multilayer processing and computer simulation of sputter deposition show that supermirror construction is approaching the capability needed to construct large neutron guides. The key remaining problem is the degree of reflectivity obtained in a single guide wall reflection. This problem is attributed to the degree of "flatness" at the atomic level that can be obtained in a multilayer supermirror. The technical objective of this project is to build guide segments that test the improvements facilitated by use of self-leveling intermetallic compounds and mechanical strain built into the layers themselves.Anticipated Results/Potential Commercial Applications as described by the awardee:The anticipated benefits from practical, thin film supermirror coatings include increased angular and energy acceptance for existing and proposed neutron guide halls. These have the direct effect of multiplying the use of thermal neutron sources with a minimal increase in construction expense. This technology also is directly applicable to a wide range of neutron and x-ray optical devices (e.g., polarizers, filters, and mirrors).

Phase II

Contract Number: ----------
Start Date: 00/00/00    Completed: 00/00/00
Phase II year
1990
Phase II Amount
$500,000
Adding neutron guides to existing and proposed thermal neutron research facilities has great economic benefit. Supermirror guides, because of their ability to conduct higher energy, shorter wavelength neutrons, are particularly attractive. Phase I demonstrated various improvements in supermirror construction technique. Specifically, using "self-leveling" intermetallic compounds and mechanical strain built into the layers significantly improved the degree of reflectivity that can be obtained in a single guide wall reflection for mirrors built to twice (2x) the critical angle of nickel coatings. Present limitations were explored by building test mirrors out to 5x. Phase II will (1) extend the useful range of high reflectivity to shorter wavelengths and higher critical angles by modifying Phase I materials and algorithms, (2) improve the capability to construct larger superrnirror neutron guide segments at higher speeds by modifying the sputtering machine, and (3) further develop those processing issues that will maximize uniformity and minimize production cost.Anticipated Results/Potential Commercial Applications as described by the awardee:Increased angular acceptance for existing and proposed neutron guides multiplies the use of thermal neutron sources with a minimal increase in expense. The availability of mirrors and collimators will also benefit neutron and x-ray instrumentation such as bomb detection by thermal neutron activation (TNA) and oil well down-pipe TNA. Room temperature thermal neutron operation is particularly desirable.