SBIR-STTR Award

Low Cost Titanium Components for Armor and Structures
Award last edited on: 4/5/02

Sponsored Program
SBIR
Awarding Agency
DOD : Army
Total Award Amount
$850,000
Award Phase
2
Solicitation Topic Code
A98-122
Principal Investigator
Vladimir Moxson

Company Information

ADMA Products Incorporated (AKA: Advance Materials Products Inc ~ ADMA Advanced Materials)

1890 Georgetown Road
Hudson, OH 44236
   (330) 650-4000
   sales@admaproducts.com
   www.admaproducts.com
Location: Single
Congr. District: 14
County: Summit

Phase I

Contract Number: DAAD17-99-C-0022
Start Date: 12/15/98    Completed: 8/9/99
Phase I year
1999
Phase I Amount
$120,000
In Phase I of the proposed program the team of ADMA Products Inc. Twinsburg OH and the University of Idaho, Moscow, ID will demonstrate the ability to produce low cost plates of Ti-6AL-4V using a powder approach with acceptable properties including ballistic behavior. At leastfour powder types will be evaluated which are potentially low cost and can also be used for the Laser Rapid Prototyping approach to titanium component fabrication. Tentatively these are (1) crushed machine turnings which will be crushed after hydrogenation, (2) CaH2 reduced TiO2, (3) powder produced by a displacement reaction (mechanical alloying) from a TiO2 or TiCl4 precursor and (4) Russian spherical plasma rotating electrode process powder. Plates will be fabricated using a low-cost loose powder sintering approach, in some cases using the thermohydrogen processing approach to enhance processability and refine the final microstructure. These plates will be evaluated for microstructureand mechanical properties, and samples supplied to the Army for ballistic testing. In a Phase I option oxygen level and microstructure will be varied, and fabricated plates evaluated. If Phase II is funded, a component tentatively selected as the Commander's Independent Thermal Viewer, MIA2 tank, will be produced using the optimum approach from Phase I.

Benefits:
The research is designed to result in production of titanium Components for Army systems as the MIA2 tank which have mechanical properties at least equivalent to current parts, but at considerably lower cost.

Phase II

Contract Number: DAAD17-01-C-0041
Start Date: 8/23/01    Completed: 8/23/03
Phase II year
2001
Phase II Amount
$730,000
In Phase I of the proposed program the term of ADMA Products Inc. Twinsburg, OH and the University of Idaho, Moscow, ID demonstrated the ability to produce low cost Ti-6A1-4V powder and are now evaluating plate produced via a powder metallurgy approach. Seven potentially low cost powder types were evaluated. (1) crushed Ti-6A1-4V machine turnings which were crushed after hydrogenation (2) crushed CP titanium turnings which were also crushed after hydrogenation, (3) Ti-6A1-4V powder produced by POLAD, Russia by direct reduction of TiO2 by CaH2, (4) powder produced from titanium sponge fines by hydrogenation-dehydrogenation (HDH) process, (5) PREP powder produced by Star Tech Metals. (6) titanium swarfs and (7) powder produced by a mechanochemical displacement reaction induced by mechanical alloying. Three of these powders were produced and evaluated at no cost to the program. Plates are being fabricated using a low-cost loose powder sintering approach. In some cases using the thermohydrogen processing approach to enhance processability and refine the final microstructure. The microstructure and mechanical properties of the plates will be determined. In the Phase I option, oxygen levels and microstructure of plates will be varied and mechanical properties of the fabricated plates will be evaluated. All of this information will be available at the time of initiation of the phase II program. In Phase II the optimum approaches from Phases I and the Phase I option will be scaled up and components tentatively selected as the Crusader Recuperator Mechanism Sleeve and Recoil Tube Sleeve plus the Bradley Fighting Vehicle Hatch, and a number of components from an internal combustion engine (valves and connecting rods) will be fabricated. In addition. plates suitable for ballistic testing will be supplied to the Army for evaluation.

Keywords:
Titanium Components Powder Metallurgy Microstructure Mechanical Properties Ballistic Behavior Cost Effective