SBIR-STTR Award

Ambient-Temperature-Storable Thermostat Resin
Award last edited on: 7/30/2014

Sponsored Program
SBIR
Awarding Agency
DOD : Army
Total Award Amount
$642,145
Award Phase
2
Solicitation Topic Code
A93-116
Principal Investigator
Clayton May

Company Information

Merlin Technologies Inc

910 American Street PO Box 1329
San Carlos, CA 94070
   (650) 591-2229
   N/A
   N/A
Location: Single
Congr. District: 14
County: San Mateo

Phase I

Contract Number: ----------
Start Date: ----    Completed: ----
Phase I year
1994
Phase I Amount
$67,050
Initial developmental research focussed on creating epoxy resinsystems which exhibited an ability to reflow several times along the pathto full cure so long as the Cure Temperature remained 20 to 30 degreesbelow the Glass Transition Temperature as the Tg fluctuated during cure.Although the process rheology is not yet fully understood, the fundamentalchemistry is sound. Demonstrated "Out-Times" of Thirty months at roomtemperature have produced prepregs with excellent track, drape, and flowwhich readily consolidate into a high-quality laminate panels which may bethermoplasticly manipulated and reshaped several times before reaching afully cured state.

Phase II

Contract Number: ----------
Start Date: ----    Completed: ----
Phase II year
1996
Phase II Amount
$575,095
Resin impregnated composite fiber reinforcements (prepregs) require nearly continuous refrigeration from the point of manufacture to consumption. Refrigeration impedes curing of the resin and therefore dominates the entire handling process. Refrigeration begins immediately after manufacture and continues until parts are made. This includes pre-shipment freezer storage, special packaging with dry ice and refrigerator trucks for transportation, and freezer storage at the user's facility. With a limited shelf life under refrigeration and a much shorter life when not refrigerated, out-time is the dominant factor in determining hoe the rate of use is managed by the end user. Unused materials must be refrozen until consumed before their shelf life expires or their out-time is exceeded, at which point prepregs are scrapped and become an environmental landfill concern. Long term ambient temperature storability of thermoset prepreg is a major factor in reducing overall costs of advanced composite structures in defense, aerospace, and commercial applications. The principles of resin chemistry which afford room temperature storage play a key role in lowering curing costs by a characteristic behavior known as solid state curing. Solid state curing will be further investigated in Phase II work.

Benefits:
Reduces handling costs; eliminates freezer costs; eliminates storage related scrapping; recyclable or convertible to other material forms on sire; greatly minimizes any waste or hazardous material disposal issues; reduces overall cost of composite materials purchased for a program. Adaptable to field repairs and battle damage repair applications.