SBIR-STTR Award

An Industrial Membrane System Suitable for Distributed Used Oil Re-Refining
Award last edited on: 9/16/2016

Sponsored Program
SBIR
Awarding Agency
DOE
Total Award Amount
$2,146,783
Award Phase
2
Solicitation Topic Code
09 c
Principal Investigator
Paul K T Liu

Company Information

Media and Process Technology Inc (AKA: MPtech~Media and Process Tech Inc)

1155 William Pitt Way
Pittsburgh, PA 15238
   (412) 826-3721
   N/A
   www.mediaandprocess.com
Location: Single
Congr. District: 17
County: Allegheny

Phase I

Contract Number: ----------
Start Date: ----    Completed: ----
Phase I year
2011
Phase I Amount
$149,972
R & D activities on membrane-based separations have been extensive in the past several decades due to the potential to provide more energy-efficient separation processes than conventional distillation, extraction, absorption, adsorption, etc. Its simplicity, essentially as an advanced filter, offers significant advantage in operation, in particular for applications, which can best be deployed through a distributed network concept, such as distributed hydrogen production promoted by US DOE recently, distributed power generation from locally available feedstocks, etc. However, commercial implementation of membrane processes in this area, though consistent with the rising national energy and environmental concerns, has lagged. Two key barriers are identified: (i) performance or material stability and reliability barriers and (ii) barrier in integrating a new membrane process into an existing process. The above barriers have limited their uses in distributed production applications, which usually deal with variable feedstocks and require operational simplicity and stability due to the lack of highly technically trained operators on-staff. Our proposed industrial membrane process system will attempt to overcome the above barriers with a focus on the use of our commercial inorganic membranes for used oil re-refining through nationwide distributed network of facilities. The performance and materials stability and integration barriers have been overcome by our proposed industrial membrane system. In this proposal we develop an innovative solution to address the remaining barrier, i.e., reliability, which is critical for a membrane system fed with variable sources of feedstock. Commercial Applications and Other

Benefits:
By re-refining waste oils, we project about 65 million barrels per year of savings potential can be achieved, resulting in about 1 to 1.5% reduction in crude imports. Recently, many new green energy sources have been developed as a result of the push by the current and previous administrations; however, the development of a high quality liquid hydrocarbon fuel and/or a replacement for liquid fuels remains a considerable challenge. Thus, any reduction in liquid hydrocarbon usage and imports via this proposed project is significant and complements the national energy technology development trend. Finally, due to the distributed generation of waste oil throughout the country, waste oil re-refining is best implemented through a distributed network of facilities.

Phase II

Contract Number: ----------
Start Date: ----    Completed: ----
Phase II year
2012
(last award dollars: 2015)
Phase II Amount
$1,996,811

Nationwide about 2.4 billion gallons of lubricants are consumed annually for automotive crankcase (about 58%), industrial processes, machine lubrication, mining, and others. About 1 billion gallons/yr is currently collected as waste oil, equivalent to1-1.5% of annual US crude oil import volume. Presently, about 9% of the collected used oil is re-refined at six facilities in US. The majority of this resource is currently burned as fuel. A report issued by the DOE in 2006 in response to The Energy Policy Act of 2005 Section 1838 highlights that the major impediment to expanding lube oil re-refining is investment costs required to design and construct new facilities for re-refining. According to the literature, about $40million in front end capital investment is required for a 30 million gallon per year (MGY) re-refining facility. This explains why the capital investment cost is listed as the primary impediment for expanding current re-refining capacity. Media and Process Technology Inc has been involved in the re-refining of waste oil using an innovative separation process which does not involve phase separation and hydrotreating as in the conventional technology. Thus, the re-refining facility can be designed and constructed in a small scale and modular operation without paying an economy of scale penalty. This not only reduces the front end capital investment per facility, but makes it uniquely suitable for regional re-refining operations to match waste oil supplies, as opposed to the conventional technology requiring a centralized operation to justify its large capital investment. A clean in place (CIP) methodology with our specially formulated cleaner package was developed to restore the flux of our ceramic membranes severely and irreversibly fouled during used oil processing, overcoming a key barrier to the commercial viability of this re-refining process. In addition, a rapid QA/QC strategy for used oil feedstock characterization and suitability for re-refining was developed. Process was demonstrated at the pilot scale in four months of continuous operation. In addition, the CIP is considered universal for oil filtration applications; several generic energy saving opportunities have been identified, which can benefit from the industrial membrane system equipped with the CIP we developed. We plan to expand our existing re-refining pilot operation to a semi-works facility to demonstrate the performance and economics of our upgraded re-refining process for petroleum-based waste oil. Then, we plan to establish the 1st regional re-refining center with our operational partner to showcase the technology and process and in parallel begin the deployment of the regional centers nationwide. Commercial Applications and Other

Benefits:
Our re-refining technology could positively impact the national energy consumption profile via an economically driven approach, potentially resulting in a 1% reduction in crude oil imports and significant reduction in air pollution and greenhouse gas emissions. Nationwide, waste oil re-refining with this technology is expected to create job opportunities. Further, the technology is readily exportable.